HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Chloroaniline → HCID 21490755, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Chloroaniline | HCID 7932 | — |
| Reactant | HCID 12593125 | HCID 12593125 | — |
| Product | HCID 21490755 | HCID 21490755 | — |
Reaction Steps
A mixture of 4-chlorohomophthalic acid (54.0 g., 0.25 mole) and m-chloroaniline (31.8 g., 0.25 mole) is heated by an oil bath until molten for two hours. When removed from the oil bath, the reaction mixture solidifies and is recrystallized twice from ethanol/ethyl acetate, giving 2-(m-Chlorophenyl)-7-chloroisoquinoline-1,3(2H,4H)-dione.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03998954 |
| Source dataset | uspto-grants-1976_12 |
| ORD ID | ord-15f772aeb4dd4f239da23998621e5168 |
| Source note | uspto-grants-1976_12 |