Methanethiol → HCID 53882703, compound

HRID 1973976Notes

Reaction equation

HRID 1973976 reaction equation
[CH3:1][O:2][C:3]1[CH:4]=[C:5]2[C:10](=[CH:11][CH:12]=1)[C:9](O)=[C:8]([CH2:14][C:15]([O:17][CH3:18])=[O:16])[CH:7]=[CH:6]2.[CH3:19][SH:20]>>[CH3:1][O:2][C:3]1[CH:4]=[C:5]2[C:10](=[CH:11][CH:12]=1)[C:9]([S:20][CH3:19])=[C:8]([CH2:14][C:15]([O:17][CH3:18])=[O:16])[CH:7]=[CH:6]2

Participants

3

Reactant 2

HCID 878MethanethiolHCID 54291935HCID 54291935, compound

Product 1

HCID 53882703HCID 53882703, compound

Procedure

By treating 25 g. of methyl 6-methoxy-1-hydroxy-2-naphthylacetate with 10 ml. of methylmercaptan as described above for the 1,6-dihydroxy compound, methyl 6-methoxy-1-methylthio-2-naphthylacetate is obtained.

Workup

  1. additionBy treating 25 g

Sources & evidence

ORD record
ord-06815f4ff1f04cac8045cf1a4f82c1ef
Source dataset
uspto-grants-1976_12
Patent number
US03998966

Reaction notes

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