HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1973999Generated: November 2, 2026
Hydroxylamine, O-ethyl- → HCID 178474708, compound
https://huagongshe.com/reaction/1973999
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Hydroxylamine, O-ethyl- | HCID 69357 | — |
| Reactant | 5-Acetyl-1,3-dimethylpyrimidine-2,4,6(1H,3H,5H)-trione | HCID 274616 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 178474708 | HCID 178474708 | — |
Reaction Steps
1.5 g of 5-acetyl-1,3-dimethylbarbituric acid was dissolved in 50 ml of ethanol and 1.5 ml of ethoxyamine was added to it. After the resulting solution was stirred at 40° C during 2 hours, it was allowed to stand at a room temperature. The separated white plates were filtered and recrystallized from ethanol, and thereby 1.4 g of the desired compound was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US03999974 |
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| Source dataset | uspto-grants-1976_12 |
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| ORD ID | ord-dd0ace17155e40818c433d3d4cdd945c |
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| Source note | uspto-grants-1976_12 |
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