Methyl iodide → HCID 20559979, compound

HRID 1974106Notes

Reaction equation

HRID 1974106 reaction equation
[CH:1]([NH:3][C:4]1[CH:9]=[CH:8][CH:7]=[CH:6][C:5]=1[CH2:10][CH:11]([C:13]1[CH:18]=[CH:17][CH:16]=[CH:15][N:14]=1)[CH3:12])=[O:2].C[I:20].[I-].[CH:22](NC1C=CC=CC=1C(C1C=CC=C[N+]=1C)(C)C)=O>>[I-:20].[CH:1]([NH:3][C:4]1[CH:9]=[CH:8][CH:7]=[CH:6][C:5]=1[CH2:10][CH:11]([C:13]1[CH:18]=[CH:17][CH:16]=[CH:15][N+:14]=1[CH3:22])[CH3:12])=[O:2]

Participants

4

Reactant 3

HCID 6328Methyl iodideHCID 20559973HCID 20559973, compoundHCID 86734321HCID 86734321, compound

Product 1

HCID 20559979HCID 20559979, compound

Procedure

Reaction of 2-[2-(2-formamidophenyl)-1-methylethyl]pyridine (24 g., 0.1 mole) with methyl iodide (28.4 g., 0.2 mole) according to the procedure of Example 2(c), affords 29.5 g. (77%) of 2-[2-(2-formamidophenyl-1-methylethyl]-1-methylpyridinium iodide, m.p. 184° - 188° C.

Workup

  1. customaffords 29.5 g

Sources & evidence

ORD record
ord-7964df23e00d49d984da20c31e970651
Source dataset
uspto-grants-1976_12
Patent number
US04000143

Reaction notes

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