HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → 2-[2-(p-Methoxybenzamido)benzyl]-1-methylpyridinium iodide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | 2'-(2-Pyridylmethyl)-p-anisanilide | HCID 20559990 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | 2-[2-(p-Methoxybenzamido)benzyl]-1-methylpyridinium iodide | HCID 20560009 | 93% |
Reaction Steps
2'-(2-Pyridylmethyl)-p-anisanilide (9.5 g., 0.03 mole) and 0.3 mole of methyl iodide in 100 ml. of acetone is refluxed with stirring for a period of 64 hr. The reaction mixture filtered and the filter cake washed with acetone provides a 93% yield of 2-[2-(p-methoxybenzamido)-benzyl]-1-methylpyridinium iodide, m.p. 184° -186° C. (corr.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04000143 |
| Source dataset | uspto-grants-1976_12 |
| ORD ID | ord-5296200d918f4e98bcc68d64d46650d3 |
| Source note | uspto-grants-1976_12 |