Formaldehyde → HCID 21488642, compound

HRID 1974142Notes

Reaction equation

[Cl:1][C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][C:3]=1[C:8](=[O:24])[C:9]1[CH:14]=[C:13]([N+:15]([O-:17])=[O:16])[CH:12]=[CH:11][C:10]=1[N:18]1[CH:22]=[N:21][N:20]=[C:19]1[CH3:23].[CH2:25]=[O:26]>>[Cl:1][C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][C:3]=1[C:8](=[O:24])[C:9]1[CH:14]=[C:13]([N+:15]([O-:17])=[O:16])[CH:12]=[CH:11][C:10]=1[N:18]1[C:19]([CH3:23])=[N:20][N:21]=[C:22]1[CH2:25][OH:26]

Participants

Reactant 2

HCID 712Formaldehyde

HCID 21488578HCID 21488578, compound

Product 1

HCID 21488642HCID 21488642, compound

Procedure

In the manner given in Example 4, 2'-chloro-5-nitro-2-(3-methyl-4H-1,2,4-triazol-4-yl)benzophenone is heated with paraformaldehyde at 125° C. to give 2'-chloro-5-nitro-2-[3-(hydroxymethyl)-5-methyl-4H-1,2,4-triazol-4-yl]benzophenone.

Sources & evidence

ORD record: ord-2d06d1aa88804ad2b7cc365d17e0e970
Source dataset: uspto-grants-1976_12
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04000153

Reaction notes

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