Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Phenethylamine → 1-beta-Phenylethylamino-6-nitroanthraquinone
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Phenethylamine | HCID 1001 | — |
| 반응물 | 1,6-Dinitroanthraquinone | HCID 74146 | — |
| 용매 | 2-Methoxyethanol | HCID 8019 | — |
| 생성물 | 1-beta-Phenylethylamino-6-nitroanthraquinone | HCID 53917138 | — |
반응 단계
15 g of 1,6-dinitroanthraquinone and 45 ml of β-phenylethylamine are stirred at 50° - 55° C (approx. 3 hours being required) until no further starting material is detectable. The mixture is diluted with 45 ml of ethylene glycol monomethyl ether whilst warm and the reaction product which separates out is filtered off at 50° C and rinsed with a little ethylene glycol monomethyl ether and water. 13.6 g of pure 1-β-phenylethylamino-6-nitroanthraquinone are obtained.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04000167 |
| 출처 데이터셋 | uspto-grants-1976_12 |
| ORD ID | ord-bc2a8e225e914c9a8efa323f14c7b4ef |
| 출처 메모 | uspto-grants-1976_12 |