Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Allyl isocyanate → 4-Isothiocyanatophenyl prop-2-en-1-ylcarbamate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Allyl isocyanate | HCID 15123 | — |
| 반응물 | Phenol, 4-isothiocyanato- | HCID 102208 | — |
| 촉매 | Triethylamine | HCID 8471 | — |
| 촉매 | Di-n-butyldilauryltin | HCID 9809426 | — |
| 용매 | Chloroform | HCID 6212 | — |
| 생성물 | 4-Isothiocyanatophenyl prop-2-en-1-ylcarbamate | HCID 21489004 | — |
반응 단계
By a procedure similar to that of Example I, the above compound (11.1 g.) in the form of a waxy solid, was prepared from 9.1 g. (0.06 m.) of p-hydroxyphenylisothiocyanate and 5.0 g. (0.06 m.) of allylisocyanate, using 35 mls. of chloroform as a solvent and 3 drops each of triethylamine and dibutyltin dilaurate as catalysts.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04000253 |
| 출처 데이터셋 | uspto-grants-1976_12 |
| ORD ID | ord-692abc3ca1aa48bc9083b601ebe9fb96 |
| 출처 메모 | uspto-grants-1976_12 |