Anthranilic Acid → HCID 13947715, compound

HRID 1974259Notes

Reaction equation

HRID 1974259 reaction equation
Cl[C:2]1[NH:3][C:4]2[CH:10]=[C:9]([CH3:11])[CH:8]=[CH:7][C:5]=2[N:6]=1.[C:12]([OH:21])(=[O:20])[C:13]1[C:14](=[CH:16][CH:17]=[CH:18][CH:19]=1)[NH2:15]>>[CH3:11][C:9]1[CH:8]=[CH:7][C:5]2[N:6]3[C:12](=[O:20])[C:13]4[C:14](=[CH:16][CH:17]=[CH:18][CH:19]=4)[N:15]=[C:2]3[NH:3][C:4]=2[CH:10]=1.[CH3:11][C:9]1[CH:8]=[CH:7][C:5]2[NH:6][C:2]3=[N:15][C:14]4[C:13]([C:12](=[O:21])[N:3]3[C:4]=2[CH:10]=1)=[CH:19][CH:18]=[CH:17][CH:16]=4

Participants

4

Reactant 2

HCID 227Anthranilic AcidHCID 116296552-chloro-6-methyl-1H-1,3-benzodiazole

Product 2

HCID 13947715HCID 13947715, compoundHCID 21489157HCID 21489157, compound

Procedure

The reaction of 2-chloro-5-methylbenzimidazole with anthranilic acid according to the procedure described in Example 1 yielded a solid mixture comprising 8-methylbenzimidazo[2,1-b]-quinazolin-12(6H)one and 9-methylbenzimidazo[2,1-b]quinazolin-12(6H)one.

Sources & evidence

ORD record
ord-25542aca9b3644d3960a032f80bd38f6
Source dataset
uspto-grants-1976_12
Patent number
US04000275

Reaction notes

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