HuagongsheHuagongshe Chemistry Print Report · For research reference only
8-chlorodibenz[b,f][1,4]oxazepine-10(11H)-carboxylic acid, hydrazide → HCID 86746507, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 8-chlorodibenz[b,f][1,4]oxazepine-10(11H)-carboxylic acid, hydrazide | HCID 13560461 | — |
| Reactant | HCID 19800028 | HCID 19800028 | — |
| Product | HCID 86746507 | HCID 86746507 | — |
Reaction Steps
8-chlorodibenz[b,f][1,4]oxazepine-10(11H)-carboxylic acid, 2-[3-[(phenylsulfonyl)amino]-1-oxopropyl]hydrazide (24) was prepared from N-(phenylsulfonyl)-β-alanine, methyl ester (23), prepared as described above in Example 23, and 8-chlorodibenz[b,f][1,4]-oxazepine-10(11H)-carboxylic acid, hydrazide (1), prepared as described above in Example 1, on a two mmol scale in the manner described in Example 18 above to yield 0.44 g (44%) of product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05283240 |
| Source dataset | uspto-grants-1994_02 |
| ORD ID | ord-931314402ce846a6922767fa39abda2c |
| Source note | uspto-grants-1994_02 |