HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,5-Dibromopentane → 1-[[(5-Bromopentyl)oxy]methyl]naphthalene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,5-Dibromopentane | HCID 8100 | — |
| Reactant | 1-Naphthalenemethanol | HCID 20908 | — |
| Product | 1-[[(5-Bromopentyl)oxy]methyl]naphthalene | HCID 19101842 | — |
Reaction Steps
1-Naphthalenemethanol (6.00 g) and 1,5-dibromopentane (11.5 ml) were treated according to the method of Intermediate 1. FCC eluting with ether-cyclohexane (1:49→2:48) gave the title compound as a colourless oil (8.41 g), t.l.c. (Cyclohexane-ether 19:1) Rf 0.22;
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05283262 |
| Source dataset | uspto-grants-1994_02 |
| ORD ID | ord-fbae953028ff4b05806115274c1026d7 |
| Source note | uspto-grants-1994_02 |