HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzoyl chloride → HCID 54451301, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzoyl chloride | HCID 7412 | — |
| Reactant | HCID 53849680 | HCID 53849680 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 54451301 | HCID 54451301 | — |
Reaction Steps
1.0 g of the product obtained in Example 8 and 2.0 ml of benzoylchloride were dissolved in 5 ml of tetrahydrofuran. Tetrahydrofuran was distilled off to a great extent and the residue was refluxed for 2 h. After cooling ether was added to the mixture and the product was filtered and triturated with ethylmethylketone. Yield 0.50 g (29%), m.p. 206°-210° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05283352 |
| Source dataset | uspto-grants-1994_02 |
| ORD ID | ord-a1e9b2060dea4822bdfa25a52fea229a |
| Source note | uspto-grants-1994_02 |