HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1974751Generated: October 31, 2026
2,6-Dimethylbenzoyl chloride → HCID 19389207, compound
https://huagongshe.com/reaction/1974751
Participants
| Role | Name | HCID | Charge |
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| Reactant | 2,6-Dimethylbenzoyl chloride | HCID 89096 | — |
| Reactant | 3,5-Dinitrocatechol | HCID 3870203 | — |
| Product | HCID 19389207 | HCID 19389207 | — |
Reaction Steps
A mixture containing 2.0 g of 3,5-dinitrocatechol in 5 ml of 2,6-dimethylbenzoylchloride was heated for 20 hours in 100° C. The excess 2,6-dimethylbenzoylchloride was removed in high vacuum. The residue was purified in silicagel column. Yield 1.5 g (45%), yellow viscous oil, which was crystallized from petroleum ether, m.p. 163°-165° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US05283352 |
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| Source dataset | uspto-grants-1994_02 |
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| ORD ID | ord-8591012c7732469d954a7a9669a1f7e2 |
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| Source note | uspto-grants-1994_02 |
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