HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phosphorus pentachloride → HCID 178444339, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phosphorus pentachloride | HCID 24819 | — |
| Reactant | HCID 178444341 | HCID 178444341 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | HCID 178444339 | HCID 178444339 | — |
Reaction Steps
In a 30 ml-reaction vessel, 2.0 g (7.3 mM) of p-(trans-4-pentylcyclohexyl)benzoic acid and 10 ml of benzene were placed. To the mixture, 1.55 g (7.4 mM) of PCl5 was added in 25 minutes to room temperature, followed by heat-refluxing for 4 hours and distilling-off of the solvent to obtain p-(trans-4-pentylcyclohexyl)benzoic acid chloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05284599 |
| Source dataset | uspto-grants-1994_02 |
| ORD ID | ord-b3995b2b992545c4b56256c129c26707 |
| Source note | uspto-grants-1994_02 |