HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethylene Glycol → 2-Hydroxyethyl nonanoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethylene Glycol | HCID 174 | — |
| Reactant | Decanoic Acid | HCID 2969 | — |
| Reactant | Lauric Acid | HCID 3893 | — |
| Reactant | Myristic Acid | HCID 11005 | — |
| Catalyst | Sulfuric Acid | HCID 1118 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | 2-Hydroxyethyl nonanoate | HCID 169334 | — |
Reaction Steps
Decanoic acid (C10 acid), dodecanoic acid (C12 acid), and tetradecanoic acid (C14 acid)-each of 100 mmol of C10, C12 and C14 acids were dissolved in 50 ml dichloromethane, and 300 mmol of ethylene glycol was added to the solutions. Several drops of H2SO4 were added to the mixture. The reaction mixtures were stored at room temperature for 9 days. Isolation of the esters were carried out using the same procedure as that to isolate ethylene glycol monopelargonate. Distillations were not undertaken.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05284819 |
| Source dataset | uspto-grants-1994_02 |
| ORD ID | ord-9b7b76631a384ba5abf1505e7fce0ace |
| Source note | uspto-grants-1994_02 |