HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylamine → HCID 19382159, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylamine | HCID 674 | — |
| Reactant | Ethyl 1-oxa-6-azaspiro[2,5]octane-6-carboxylate | HCID 13672926 | — |
| Product | HCID 19382159 | HCID 19382159 | — |
Reaction Steps
5.2 g (28 mmol) of ethyl 6-aza-1-oxaspiro[2,5]octane-6-carboxylate are added dropwise to 30 ml of dimethylamine solution (40% in water) and the mixture is stirred overnight at room temperature. It is then concentrated and distilled.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05284842 |
| Source dataset | uspto-grants-1994_02 |
| ORD ID | ord-2859e2d675904ab5aec506ce4be8a520 |
| Source note | uspto-grants-1994_02 |