HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 19382165, compound → 3-(Methoxymethyl)pyrrolidin-3-ol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 19382165 | HCID 19382165 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | 3-(Methoxymethyl)pyrrolidin-3-ol | HCID 21918851 | — |
Reaction Steps
10 g (45 mmol) of 1-benzyl-3-hydroxy-3-methoxymethylpyrrolidine are hydrogenated using 3 g of Pd/active carbon (10% Pd) in 200 ml of methanol at 100° C. and 100 bar. The catalyst is filtered off with suction, the filtrate is concentrated and the residue is distilled.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05284842 |
| Source dataset | uspto-grants-1994_02 |
| ORD ID | ord-d26a551e7870428485d0f6560aff2047 |
| Source note | uspto-grants-1994_02 |