HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenethylamine → HCID 19382195, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenethylamine | HCID 1001 | — |
| Reactant | 5-Benzyl-1-oxa-5-azaspiro[2.4]heptane | HCID 11194805 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 19382195 | HCID 19382195 | — |
Reaction Steps
18.2 g (95 mmol) of 5-benzyl-1-oxa-5-azaspiro[2,4]heptane are added dropwise to 15.6 ml (0.115 mol) of benzylmethylamine in 300 ml of water and the mixture is stirred for 15 hours at room temperature. The product is extracted using CH2Cl2, the extracts are dried using K2CO3 and concentrated, and incipient distillation is carried out up to 160° C. (oil bath temperature).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05284842 |
| Source dataset | uspto-grants-1994_02 |
| ORD ID | ord-ea13bff5735b4be288f75c7fa6f2f896 |
| Source note | uspto-grants-1994_02 |