HuagongsheHuagongshe Chemistry Print Report · For research reference only
Azocan → HCID 54496313, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Azocan | HCID 14276 | — |
| Reactant | HCID 22874407 | HCID 22874407 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 54496313 | HCID 54496313 | 86.8% |
Reaction Steps
Benzyl (2R)-2-carboxymethyl-4-methylvalerate (320 mg), octahydroazocin (165 mg) and WSCD·HCl (280 mg) were reacted in methylene chloride (20 ml) in a similar manner to that of Preparation 18 to give benzyl (2R)-2-(octahydroazocin-1-ylcarbonylmethyl)-4-methylvalerate (378 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05284828 |
| Source dataset | uspto-grants-1994_02 |
| ORD ID | ord-e7583037fcdc4a7fa2817da87c9059d0 |
| Source note | uspto-grants-1994_02 |