Methyl iodide → 131988-14-2

HRID 1975092Notes

Reaction equation

HRID 1975092 reaction equation
[CH3:1][I:2].[CH2:3]([O:7][C:8]1[C:9]([C:13]2[CH:14]=[N:15][CH:16]=[CH:17][CH:18]=2)=[N:10][S:11][N:12]=1)[CH2:4][CH2:5][CH3:6]>CC(C)=O>[I-:2].[CH2:3]([O:7][C:8]1[C:9]([C:13]2[CH:14]=[N+:15]([CH3:1])[CH:16]=[CH:17][CH:18]=2)=[N:10][S:11][N:12]=1)[CH2:4][CH2:5][CH3:6]

Participants

4

Reactant 2

HCID 6328Methyl iodideHCID 15180133HCID 15180133, compound

Product 1

HCID 19075249131988-14-2

Reagents, catalysts & solvents 1

HCID 180AcetoneSolvent

Procedure

A mixture of methyl iodide (0.3 ml, 5 mmol) and 3-(4-butoxy-1,2,5-thiadiazol-3-yl)pyridine (580 mg, 2.5 mmol) in acetone (5 ml) was stirred at room temperature for 18 h. The title compound precipitated from the solution and was collected by filtration to yield 0.60 g (64%).

Workup

  1. customThe title compound precipitated from the solution
  2. filtrationwas collected by filtration
  3. customto yield 0.60 g (64%)

Sources & evidence

ORD record
ord-3d37c2009efd4ce1b182838ce37a4d8d
Source dataset
uspto-grants-1994_02
Patent number
US05284859

Reaction notes

Loading…