Methyl iodide → HCID 19075349, compound

HRID 1975105Notes

Reaction equation

HRID 1975105 reaction equation
[CH3:1][I:2].[CH2:3]([O:7][C:8]1[C:9]([C:13]2[CH:14]=[N:15][CH:16]=[CH:17][CH:18]=2)=[N:10][S:11][N:12]=1)[CH2:4][CH:5]=[CH2:6]>CC(C)=O>[I-:2].[CH2:3]([O:7][C:8]1[C:9]([C:13]2[CH:14]=[N+:15]([CH3:1])[CH:16]=[CH:17][CH:18]=2)=[N:10][S:11][N:12]=1)[CH2:4][CH:5]=[CH2:6]

Participants

4

Reactant 2

HCID 6328Methyl iodideHCID 19075515HCID 19075515, compound

Product 1

HCID 19075349HCID 19075349, compound

Reagents, catalysts & solvents 1

HCID 180AcetoneSolvent

Procedure

A mixture of methyl iodide (0.5 ml, 7.5 mmol) and 3-(4(3-butenyloxy)-1,2,5-thiadiazol-3-yl)pyridin (583 mg, 2.5 mmol) in acetone (5 ml) was stirred at room temperature for 18 h. The title compound precipitated from the solution and was collected by filtration to yield 890 mg (96%).

Workup

  1. customThe title compound precipitated from the solution
  2. filtrationwas collected by filtration
  3. customto yield 890 mg (96%)

Sources & evidence

ORD record
ord-321de37948bb4e77a395427207d159fe
Source dataset
uspto-grants-1994_02
Patent number
US05284859

Reaction notes

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