Methyl iodide → 3-(3-(2-(2-Butoxyethoxy) ethoxy)-1,2,5-thiadiazol-4-yl)-1-methylpyridinium iodide

HRID 1975153Notes

Reaction equation

HRID 1975153 reaction equation
[CH3:1][I:2].[CH2:3]([O:7][CH2:8][CH2:9][O:10][CH2:11][CH2:12][O:13][C:14]1[C:15]([C:19]2[CH:20]=[N:21][CH:22]=[CH:23][CH:24]=2)=[N:16][S:17][N:18]=1)[CH2:4][CH2:5][CH3:6]>CC(C)=O>[I-:2].[CH2:3]([O:7][CH2:8][CH2:9][O:10][CH2:11][CH2:12][O:13][C:14]1[C:15]([C:19]2[CH:20]=[N+:21]([CH3:1])[CH:22]=[CH:23][CH:24]=2)=[N:16][S:17][N:18]=1)[CH2:4][CH2:5][CH3:6]

Participants

4

Reactant 2

HCID 6328Methyl iodideHCID 190753243-(3-(2-(2-Butoxyethoxy)ethoxy)-1,2,5-thiadiazol-4-yl)pyridine

Product 1

HCID 190752543-(3-(2-(2-Butoxyethoxy) ethoxy)-1,2,5-thiadiazol-4-yl)-1-methylpyridinium iodide

Reagents, catalysts & solvents 1

HCID 180AcetoneSolvent

Procedure

A mixture of methyl iodide (0.5 ml, 9 mmol) and 3-(4-(2-(2-butoxyethoxy) ethoxy)-1,2,5-thiadiazol-3-yl)pyridine (3 mmol) in acetone (5 ml) was stirred at room temperature for 18 h. The title compound precipitated from the solution and was collected by filtration.

Workup

  1. customThe title compound precipitated from the solution
  2. filtrationwas collected by filtration

Sources & evidence

ORD record
ord-312294e84d464086b040856be371ce59
Source dataset
uspto-grants-1994_02
Patent number
US05284859

Reaction notes

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