HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → 3-(3-(4-Methylpiperidino)-1,2,5-thiadiazol-4-yl)-1-methylpyridinium iodide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | 3-(3-(4-Methylpiperidino)-1,2,5-thiadiazol-4-yl)pyridine | HCID 19075317 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | 3-(3-(4-Methylpiperidino)-1,2,5-thiadiazol-4-yl)-1-methylpyridinium iodide | HCID 19075375 | — |
Reaction Steps
A mixture of methyl iodide (0.5 ml, 8 mmol) and 3-(4-(4-methylpiperidino)-1,2,5-thiadiazol-3-yl) pyridine (0.8 g, 3.1 mmol) in acetone (5 ml) was stirred at room temperature for 18 h. The title compound precipitated from the solution and was collected by filtration to yield 1.14 g (92%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05284859 |
| Source dataset | uspto-grants-1994_02 |
| ORD ID | ord-0e877927317d4ae488537b2c0d9c1465 |
| Source note | uspto-grants-1994_02 |