Methyl iodide → HCID 19075272, compound

HRID 1975186Notes

Reaction equation

HRID 1975186 reaction equation
[CH3:1][I:2].[CH2:3]([S:8][C:9]1[C:10]([C:14]2[CH:15]=[N:16][CH:17]=[CH:18][CH:19]=2)=[N:11][S:12][N:13]=1)[CH2:4][CH2:5][CH2:6][CH3:7]>>[I-:2].[CH2:3]([S:8][C:9]1[C:10]([C:14]2[CH:15]=[N+:16]([CH3:1])[CH:17]=[CH:18][CH:19]=2)=[N:11][S:12][N:13]=1)[CH2:4][CH2:5][CH2:6][CH3:7]

Participants

3

Procedure

Methyl iodide (0.5 ml, 7.5 mmol) was added to a solution of 3-(4-pentylthio-1,2,5-thiadiazol-3-yl)pyridine (3 mmol) and the reaction mixture was stirred at room temperature for 48 h and evaporated.

Workup

  1. customevaporated

Sources & evidence

ORD record
ord-1238d172b24d40f99520efb1bbc7fff9
Source dataset
uspto-grants-1994_02
Patent number
US05284859

Reaction notes

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