HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethylenediamine → Dimethyl ethane-1,2-diylbiscarbamate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethylenediamine | HCID 3301 | — |
| Reactant | Dimethyl Carbonate | HCID 12021 | — |
| Product | Dimethyl ethane-1,2-diylbiscarbamate | HCID 235151 | — |
Reaction Steps
Ethylene diamine (6 g) and dimethyl carbonate (18 g) were mixed together in a round bottom flask at 20° C. TBD (0.1 g) was added and the mixture allowed to stand for 24h. After this time a white solid product was collected and recrystallised from methanol to give bis (methoxycarbonyl) ethylene diamine. NMR and IR spectra were consistent with the desired compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05286265 |
| Source dataset | uspto-grants-1994_02 |
| ORD ID | ord-b88e3aefaf0548b0a72986350e6316af |
| Source note | uspto-grants-1994_02 |