1-Methylimidazole → HCID 178480866, compound

HRID 1975465Notes

Reaction equation

HRID 1975465 reaction equation
[Br:1][CH2:2][CH2:3][CH2:4][C:5]#[N:6].[CH3:7][N:8]1[CH:12]=[CH:11][N:10]=[CH:9]1>C1C=CC=CC=1>[Br-:1].[CH3:7][N:8]1[CH:12]=[CH:11][N+:10]([CH2:2][CH2:3][CH2:4][C:5]#[N:6])=[CH:9]1

Participants

4

Reactant 2

HCID 13901-MethylimidazoleHCID 214124-Bromobutyronitrile

Product 1

HCID 178480866HCID 178480866, compound

Reagents, catalysts & solvents 1

HCID 241BenzeneSolvent

Conditions

Temperature
60 °C

Procedure

A mixture of 4-bromobutyronitrile (5.6 g) and 1-methylimidazole (3.0 ml) in benzene (20 ml) was heated to 60° C. for 6 hours. The resulting syrup was separated by decantation, washed with ether and dried to give 4-(3-methyl-1-imidazolio)butyronitrile bromide (7.43 g).

Workup

  1. customThe resulting syrup was separated by decantation
  2. washwashed with ether
  3. customdried

Sources & evidence

ORD record
ord-bdd156e36e9f4c76a16cf334132296f7
Source dataset
uspto-grants-1994_02
Patent number
US05286721

Reaction notes

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