HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl 2-((3-nitrophenyl)methylene)-3-oxobutanoate → HCID 19100193, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl 2-((3-nitrophenyl)methylene)-3-oxobutanoate | HCID 1536427 | — |
| Reactant | 3-[4-(1-Imidazolylmethyl)phenyl]-2-propen-1-yl 3-aminocrotonate | HCID 86747583 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 19100193 | HCID 19100193 | — |
Reaction Steps
2.97 g (10 mM) of 3-[4-(1-imidazolylmethyl)phenyl]-2-propen-1-yl 3-aminocrotonate and 2.49 g (10 mM) of methyl 2-(3-nitrobenzylidene)acetoacetate were dissolved in 50 ml of toluene and then the solution was refluxed for eight hours. After cooling, the crystals were filtered off and then recrystallized from methanol whereby the captioned compound was obtained. The yield was 4.01 g (76%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05286869 |
| Source dataset | uspto-grants-1994_02 |
| ORD ID | ord-7c5b63ea122245a3b43f19fcc95a401c |
| Source note | uspto-grants-1994_02 |