HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Methoxyethyl 2-((3-nitrophenyl)methylene)acetoacetate → HCID 86747586, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Methoxyethyl 2-((3-nitrophenyl)methylene)acetoacetate | HCID 3016087 | — |
| Reactant | 3-[4-(1-Imidazolylmethyl)phenyl]-2-propen-1-yl 3-aminocrotonate | HCID 86747583 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 86747586 | HCID 86747586 | — |
Reaction Steps
297 mg (1 mM) of 3-[4-(1-imidazolylmethyl)phenyl]-2-propen-1-yl 3-aminocrotonate and 293 mg (1 mM) of 2-methoxyethyl 2-(3-nitrobenzylidene)acetoacetate were dissolved in 5 ml of toluene and refluxed for six hours. After cooling, the crystals produced were filtered off and recrystallized from methanol whereby the captioned compound was obtained. The yield was 502 mg (87.6%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05286869 |
| Source dataset | uspto-grants-1994_02 |
| ORD ID | ord-bf7a96b3460649c082339778fc60b1a0 |
| Source note | uspto-grants-1994_02 |