HuagongsheHuagongshe Chemistry Print Report · For research reference only
Terephthalaldehyde → HCID 354777, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Terephthalaldehyde | HCID 12173 | — |
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | Acetylacetone | HCID 31261 | — |
| Solvent | Isopropanol | HCID 3776 | — |
| Product | HCID 354777 | HCID 354777 | — |
Reaction Steps
To a mixture containing 1.34 g of 1,4-benzenedicarboxaldehyde and 2.1 g of 2,4-pentanedione in 20ml of 2-propanol was gradually added 3.0 g of thionyl chloride with stirring and cooling below 20° C. The mixture was stirred over night at room temperature, filtered and washed with 2-propanol. Yield 1.1 g (55%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05288750 |
| Source dataset | uspto-grants-1994_02 |
| ORD ID | ord-44d97cc1a5644d1a8a1055a8eaf503a2 |
| Source note | uspto-grants-1994_02 |