HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetylacetone → HCID 12128919, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetylacetone | HCID 31261 | — |
| Reactant | 4-(Trifluoromethyl)benzaldehyde | HCID 67996 | — |
| Product | HCID 12128919 | HCID 12128919 | — |
Reaction Steps
4-Trifluoromethylbenzaldehyde (8,7 g) was condensed with 2,4-pentanedione (5,01 g) in a similar manner as described above. The crude product was crystallized from a mixture of ether-petroleum ether (1:1), mp 46°-48° C., yield 3.8 g (30%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05288750 |
| Source dataset | uspto-grants-1994_02 |
| ORD ID | ord-f0c8f933fd054718b5237cd28bb405d7 |
| Source note | uspto-grants-1994_02 |