HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetylacetone → HCID 14044541, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetylacetone | HCID 31261 | — |
| Reactant | 4-Methyloxybenzyl chloride | HCID 69993 | — |
| Product | HCID 14044541 | HCID 14044541 | — |
Reaction Steps
4-methoxybenzyl chloride was condensed with 2,4-pentanedione as described in Example 6 to give 3-(4-methoxybenzyl)-2,4-pentanedione as an yellow oil. The crude product was treated first with bromine and then with pyridine as described in Example 12 to give the title compound, Mp 71°-72° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05288750 |
| Source dataset | uspto-grants-1994_02 |
| ORD ID | ord-9664eb1ff8264c5b863f9c7a4895a043 |
| Source note | uspto-grants-1994_02 |