HuagongsheHuagongshe Chemistry Print Report · For research reference only
Azobisisobutyronitrile → HCID 19098804, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Azobisisobutyronitrile | HCID 6547 | — |
| Reactant | N-bromobutanimide | HCID 67184 | — |
| Reactant | HCID 826643 | HCID 826643 | — |
| Product | HCID 19098804 | HCID 19098804 | — |
Reaction Steps
The synthesis of this compound proceeded in the same fashion as in Example 11 using 24.93 g (0.075 mol) of 5-methyl-benzene-1,3-diol dibenzoate, a catalytic amount of 2,2'-azobisisobutyronitrile and 13.35 g (0.075 mol) of N-bromosuccinimide. Recrystallization of the crude material from ethyl acetate gave a product (m.p. 123°-126° C.) which was used directly in the next step.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05288871 |
| Source dataset | uspto-grants-1994_02 |
| ORD ID | ord-5f1f2e0353584f07b75175da2d6b9dff |
| Source note | uspto-grants-1994_02 |