Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Styrene | HCID 7501 | — |
| Reactant | Propylene Carbonate | HCID 7924 | — |
| Reactant | Chlorobenzene | HCID 7964 | — |
| Reactant | Sodium Carbonate | HCID 10340 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | Stilbene | HCID 11502 | — |
Reaction Steps
Under argon, a solution containing 122 mg of chlorobenzene, 229 mg of sodium carbonate, 141 mg of styrene and 1 ml of propylene carbonate stabilized colloid solution with a palladium content of 4.023 mg is heated at 155° C. with stirring in a sealed vessel for 65 h. At the end of the reaction, 2 ml of diethyl ether is added, and the mixture is filtered. The yield of desired product as determined by GC is 34%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US06224739B1 |
|---|
| Source dataset | uspto-grants-2001_05 |
|---|
| ORD ID | ord-a77d0667cbc744f485128a561c188b59 |
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| Source note | uspto-grants-2001_05 |
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