Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Styrene | HCID 7501 | — |
| Reactant | Propylene Carbonate | HCID 7924 | — |
| Reactant | Chlorobenzene | HCID 7964 | — |
| Reactant | Sodium Carbonate | HCID 10340 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | Stilbene | HCID 11502 | — |
Reaction Steps
Under argon, a solution containing 122 mg of chlorobenzene, 106 mg of sodium carbonate, 157 mg of styrene and 1 ml of propylene carbonate stabilized 0.001 M colloid solution is heated at 155° C. with stirring in a sealed vessel for 17 h. At the end of the reaction, 2 ml of diethyl ether is added, and the mixture is filtered. The yield of isolated trans-stilbene is 15%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US06224739B1 |
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| Source dataset | uspto-grants-2001_05 |
|---|
| ORD ID | ord-be6cd414ea7c4557a3de9d5e797aa181 |
|---|
| Source note | uspto-grants-2001_05 |
|---|
