HuagongsheHuagongshe Chemistry Print Report · For research reference only
N5-(iminomethoxymethyl)-L-ornithine dihydrochloride → HCID 178475098, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N5-(iminomethoxymethyl)-L-ornithine dihydrochloride | HCID 86583873 | — |
| Reactant | HCID 178475096 | HCID 178475096 | — |
| Product | HCID 178475098 | HCID 178475098 | 94% |
Reaction Steps
By the method described above for the preparation of N5-(iminomethoxymethyl)-L-ornithine dihydrochloride, 0.78 g (1.97 mmol) N2-(tert-butoxycarbonyl)-N5-(ethoxyiminomethyl)-L-ornithine tert-butyl ester hydrochloride was deprotected to yield 0.51 g (94%) N5-(ethoxyiminomethyl)-L-ornithine dihydrochloride monohydrate. TLC (silica gel, ammonium hydroxide:methanol/1/25) Rf=0.24. Mass spectrum (CI) 204 (MH+, 74%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06225305B1 |
| Source dataset | uspto-grants-2001_05 |
| ORD ID | ord-648373a62dc045b0b9908c1597010e07 |
| Source note | uspto-grants-2001_05 |