Propyl Isothiocyanate → HCID 21999981, compound

HRID 1975914Notes

Reaction equation

HRID 1975914 reaction equation
[C:1]([C:3]1[C:4]([S:15]([NH2:18])(=[O:17])=[O:16])=[C:5]([NH:9][C:10]([O:12][CH2:13][CH3:14])=[O:11])[S:6][C:7]=1[CH3:8])#[N:2].[CH2:19]([N:22]=[C:23]=[S:24])[CH2:20][CH3:21]>>[C:1]([C:3]1[C:4]([S:15]([NH:18][C:23]([NH:22][CH2:19][CH2:20][CH3:21])=[S:24])(=[O:16])=[O:17])=[C:5]([NH:9][C:10]([O:12][CH2:13][CH3:14])=[O:11])[S:6][C:7]=1[CH3:8])#[N:2]

Participants

3

Reactant 2

HCID 69403Propyl IsothiocyanateHCID 21999991HCID 21999991, compound

Product 1

HCID 21999981HCID 21999981, compound

Procedure

The title compound was prepared from 4-cyano-2-ethoxycarbonylamino-5-methyl-thiophene-3-sulfonamide and propyl isothiocyanate in analogy with the synthesis described in Example 1-d; m.p. 167-168° C.

Sources & evidence

ORD record
ord-397a172f622647b09df97751eefea1ec
Source dataset
uspto-grants-2001_05
Patent number
US06225310B1

Reaction notes

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