Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Cyclopentyl isothiocyanate → N-[5-Chloro-3-(cyclopentylthiocarbamoyl)sulfamoylthiophen-2-yl]acetamide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Cyclopentyl isothiocyanate | HCID 141792 | — |
| 반응물 | N-(5-chloro-3-sulfamoylthiophen-2-yl)-acetamide | HCID 22000000 | — |
| 생성물 | N-[5-Chloro-3-(cyclopentylthiocarbamoyl)sulfamoylthiophen-2-yl]acetamide | HCID 21999997 | — |
반응 단계
The title compound was prepared from N-(5-chloro-3-sulfamoylthiophen-2-yl)-acetamide and cyclopentyl isothiocyanate by a procedure analogous to the procedure described in example 15a (yield of crude product: 93%); 1H-NMR (DMSO-d6): δ1.3-2.0 (m, 8H, (CH2)4), 2.28 (s, 3H, CH3), 4.32 (sext, 1H, CH), 7.16 (s, 1H, H-4), 8.48 (br d, 1H, NH), 10.23 (br s, 1H, NH).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06225310B1 |
| 출처 데이터셋 | uspto-grants-2001_05 |
| ORD ID | ord-54ab9b7d65824b2a83913917efb5b319 |
| 출처 메모 | uspto-grants-2001_05 |