HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Bromoheptane → 7-(1-Adamantyl)-6-heptyloxy-2-bromonaphthalene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Bromoheptane | HCID 12369 | — |
| Reactant | 3-(Adamantan-1-yl)-6-bromonaphthalen-2-ol | HCID 14549072 | — |
| Product | 7-(1-Adamantyl)-6-heptyloxy-2-bromonaphthalene | HCID 22000295 | 79% |
Reaction Steps
Following the procedure of Example 8(b), but reacting 3.4 g (9.5 mmol) of 3-(1-adamantyl)-6-bromo-2-naphthol with 2.05 g (11.4 mmol) of 1-bromoheptane, 3.4 g (79%) of 7-(1-adamantyl)-6-heptyloxy-2-bromonaphthalene were obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06225328B1 |
| Source dataset | uspto-grants-2001_05 |
| ORD ID | ord-e8d1272caf4a47d58cc0af2e8c2488bc |
| Source note | uspto-grants-2001_05 |