HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl 5-bromovalerate → HCID 70230620, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl 5-bromovalerate | HCID 84580 | — |
| Reactant | HCID 22000346 | HCID 22000346 | — |
| Product | HCID 70230620 | HCID 70230620 | 65.4% |
Reaction Steps
Following the procedure of Example 12(a), but reacting 2 g (4.5 mmol) of allyl 4-[7-(1-adamantyl)-6-hydroxy-2-naphthyl]benzoate with 1.4 g (6.7 mmol) of ethyl 5-bromovalerate, 1.55 g (59%) of the expected compound was obtained, which compound had a melting point of 117°-8° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06225328B1 |
| Source dataset | uspto-grants-2001_05 |
| ORD ID | ord-c8a4fe68090f45b4be300ad2c9403d23 |
| Source note | uspto-grants-2001_05 |