HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-[(2-phenylbenzoyl)amino]benzoic Acid → (3aR)-5-[4-[(2-Phenylbenzoyl) Amino]Benzoyl]-1,2,3,3a,4,5-Hexahydro-Pyrrolo[1,2-a]Quinoxaline
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-[(2-phenylbenzoyl)amino]benzoic Acid | HCID 10543502 | — |
| Reactant | (R)-1,2,3,3A,4,5-hexahydropyrrolo[1,2-a]quinoxaline | HCID 40639603 | — |
| Product | (3aR)-5-[4-[(2-Phenylbenzoyl) Amino]Benzoyl]-1,2,3,3a,4,5-Hexahydro-Pyrrolo[1,2-a]Quinoxaline | HCID 59954337 | 57.8% |
Reaction Steps
The same procedures used in Example 1 were repeated using (3aR)-1,2,3,3a,4,5-hexahydro-pyrrolo[1,2-a]quinoxaline prepared in Reference Example 15 and 4-[(2-phenylbenzoyl)amino]benzoic acid to give the title compound after recrystallization from dioxane-hexane. Yield 57.8%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06225306B1 |
| Source dataset | uspto-grants-2001_05 |
| ORD ID | ord-253f2d8cdf2b4349aea55454476a3c7a |
| Source note | uspto-grants-2001_05 |