HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → 1,2,3,6-Tetrahydro-1-methyl-4-(2,4,6-trimethoxyphenyl)-3-pyridinol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | HCID 9866952 | HCID 9866952 | — |
| Product | 1,2,3,6-Tetrahydro-1-methyl-4-(2,4,6-trimethoxyphenyl)-3-pyridinol | HCID 9925657 | — |
Reaction Steps
treating the reaction mixture containing the compound (VI) directly with water and reacting by stirring at 50°-100° C., preferably at 60°-80° C., to give 3(R,S)-hydroxy-1-methyl4-(2,4,6-trimethoxyphenyl)-1,2,3,6-tetrahydropyridine (VII), and
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06225473B1 |
| Source dataset | uspto-grants-2001_05 |
| ORD ID | ord-f260aa7d90794869aa5c027989fdd3f5 |
| Source note | uspto-grants-2001_05 |