HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl D-alaninate hydrochloride → HCID 54488601, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl D-alaninate hydrochloride | HCID 11182647 | — |
| Reactant | 4-But-2-ynyloxy-benzenesulfonyl chloride | HCID 11195928 | — |
| Product | HCID 54488601 | HCID 54488601 | — |
Reaction Steps
According to the procedure of Example 20, 0.500 g (3.58 mmol) of D-alanine methyl ester hydrochloride and 0.877 g (3.58 mmol) of 4but-2-ynyloxybenzenesulfonyl chloride provided 0.532 g of the NH-sulfonamide ester, (2R)-2-(4-but-2-ynyloxy-benzenesulfonylamino)-propionic acid methyl ester, as a white solid. Electrospray Mass Spec 312.1 (M+H)+
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06225311B1 |
| Source dataset | uspto-grants-2001_05 |
| ORD ID | ord-7e990b955d1d469c93fb4b46e6da13d4 |
| Source note | uspto-grants-2001_05 |