HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Water → 4-N,N-dimethylaminophenylacetic acid
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Water | HCID 962 | — |
| Edukt | 2,2'-Diazenediylbis(2-methylpropanimidamide) | HCID 1969 | — |
| Edukt | Methyl Chloride | HCID 6327 | — |
| Edukt | Acrylamide | HCID 6579 | — |
| Edukt | Dimethylaminopropylacrylamide | HCID 18359659 | — |
| Produkt | 4-N,N-dimethylaminophenylacetic acid | HCID 152203 | — |
Reaktionsschritte
CH3CL/dimethylaminopropylacrylamide, quaternized with methyl chloride, and 29 g of acrylamide were added to 541 g of water with 200 mg azo-bisisobutyroamidine (AIBA) and after passage of nitrogen therethrough, the mixture was irradiated for 30 minutes by an Osram HWL 250-W lamp. The gel so obtained was dried to a residual water content of 9% and ground.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US06228964B1 |
| Quelldatensatz | uspto-grants-2001_05 |
| ORD ID | ord-b975593d5010421ea0038864bc29a1c2 |
| Quellennotiz | uspto-grants-2001_05 |