HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Bromoethanol → HCID 18316809, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Bromoethanol | HCID 10898 | — |
| Reactant | Sodium Bicarbonate | HCID 516892 | — |
| Reactant | 3-(n-butylamino)phenol | HCID 11126626 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 18316809 | HCID 18316809 | 54% |
Reaction Steps
0.1 mol of 3-(n-butylamino)phenol in 100 ml of methanol is heated under reflux for 10 h with 0.11 mol of 2-bromoethanol and 0.1 mol of NaHCO3. After cooling, the reaction mixture is filtered, the solvent removed under reduced pressure and the residue fractionated to give 3-[N-(n-butyl)-N-(2-hydroxyethyl)amino]phenol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06228977B1 |
| Source dataset | uspto-grants-2001_05 |
| ORD ID | ord-8221903618a64b1b930234bb44968494 |
| Source note | uspto-grants-2001_05 |