HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Aminophenol → HCID 18316812, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Aminophenol | HCID 11568 | — |
| Reactant | 1-Bromoheptane | HCID 12369 | — |
| Reactant | Sodium Bicarbonate | HCID 516892 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 18316812 | HCID 18316812 | 62% |
Reaction Steps
One-tenth mol of m-aminophenol in 150 ml of methanol is treated with 0.11 mol of n-heptyl bromide and 0.1 mol of NaHCO3 and the mixture is heated under reflux for 5 h. After cooling, the reaction mixture is filtered and the solvent removed under reduced pressure. The residual oil is vacuum fractionated to give 3-(n-heptylamino)phenol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06228977B1 |
| Source dataset | uspto-grants-2001_05 |
| ORD ID | ord-7ef15e214e374c33a4842931dd135a1c |
| Source note | uspto-grants-2001_05 |