HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylformamide → HCID 53937558, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylformamide | HCID 6228 | — |
| Reactant | Oxalyl chloride | HCID 65578 | — |
| Reactant | HCID 21705592 | HCID 21705592 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 53937558 | HCID 53937558 | — |
Reaction Steps
A solution of (15.1 mmol) of the product from Step E in 73 mL of dichloromethane is treated with 1.4 mL (17 mmol, 1.1 equivalents) of oxalyl chloride and 0.02 mL (0.3 mmol, 0.02 equivalents) of dimethylformamide at ambient temperature, causing some bubbling, and is stirred overnight. The resulting solution of the title compound is used in step G without isolation.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06229025B1 |
| Source dataset | uspto-grants-2001_05 |
| ORD ID | ord-b4ffcceb6f88427daa6d814f73c07cba |
| Source note | uspto-grants-2001_05 |