HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylformamide → HCID 54374693, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylformamide | HCID 6228 | — |
| Reactant | Oxalyl chloride | HCID 65578 | — |
| Reactant | HCID 21705576 | HCID 21705576 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 54374693 | HCID 54374693 | — |
Reaction Steps
A solution of 15.1 mmoles of the product from Step E in 73 mL of dichloromethane is treated with 1.4 mL (17 mmol, 1.1 equivalents) of oxalyl chloride and 0.02 mL (0.3 mmol, 0.02 equivalents) of dimethylformamide at ambient temperature, causing some bubbling, and is stirred overnight. The resulting solution of the title compound is used in step G without isolation.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06229025B1 |
| Source dataset | uspto-grants-2001_05 |
| ORD ID | ord-4cb6b14ae0f14e17a27e5a10340ee937 |
| Source note | uspto-grants-2001_05 |