Sodium borohydride → HCID 21999515, compound

HRID 1976933Notes

Reaction equation

[CH3:1][N:2]([CH3:13])[C:3]1[C:9]([F:10])=[CH:8][C:6](N)=[C:5]([O:11][CH3:12])[CH:4]=1.[BH4-].[Na+]>>[CH3:13][N:2]([CH3:1])[C:3]1[CH:4]=[C:5]([O:11][CH3:12])[CH:6]=[CH:8][C:9]=1[F:10]

Participants

Reactant 2

HCID 4311764Sodium borohydride

HCID 21999507HCID 21999507, compound

Product 1

HCID 21999515HCID 21999515, compound

Procedure

Using general method D, the product from Example 20 is diazotized and reduced with sodium borohydride to give Compound 21.

Sources & evidence

ORD record: ord-786c0942227a4495b60cb1238b0a9540
Source dataset: uspto-grants-2001_05
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US06229055B1

Reaction notes

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