HuagongsheHuagongshe Chemistry Print Report · For research reference only
L-Phenylalanine → HCID 86756690, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | L-Phenylalanine | HCID 6140 | — |
| Reactant | Tert-butyl 4-(2-hydroxyethyl)piperazine-1-carboxylate | HCID 735736 | — |
| Product | HCID 86756690 | HCID 86756690 | 78% |
Reaction Steps
N-(2-Chloro-6-methylbenzoyl)-4-[(2,6-dichlorophenyl)carbonyl]amino]-L-phenylalanine 2-[4-[(1,1-dimethylethoxy)carbonyl]-1-piperazinyl]ethyl ester was prepared in 78% yield from N-(2-chloro-6-methylbenzoyl)4-[(2,6-dichlorophenyl)carbonyl]amino]-L-phenylalanine and 2-[4-[(1,1-dimethylethoxy)carbonyl]-1-piperazinyl]ethanol using the procedure described in example 129. HR MS: Obs. mass, 717.1995. Calcd. mass, 717.2013 (M+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06229011B1 |
| Source dataset | uspto-grants-2001_05 |
| ORD ID | ord-f8d13e6d79c3487ebae2abee22e25ffb |
| Source note | uspto-grants-2001_05 |