Allyl bromide → HCID 21997116, compound
Reaction equation
[C:1]([O:6][CH:7](OCC=C)[CH2:8][C:9]1[CH:14]=[CH:13][CH:12]=[CH:11][CH:10]=1)(=[O:5])[C:2]([CH3:4])=[CH2:3].[CH2:19]([O:22]C1C=CC(CCO)=CC=1)[CH:20]=[CH2:21].C(Br)C=C>>[C:1]([O:6][CH2:7][CH2:8][C:9]1[CH:10]=[CH:11][C:12]([O:22][CH2:19][CH:20]=[CH2:21])=[CH:13][CH:14]=1)(=[O:5])[C:2]([CH3:4])=[CH2:3]Participants
4
Procedure
Allyloxyphenethyl methacrylate, 82% purity, was prepared in the manner of Example 3 from 2-(4-allyloxyphenyl)ethyl alcohol. The starting 2-(4-allyloxyphenyl)ethyl alcohol was prepared by alkylation of the corresponding phenolic alcohol with allyl bromide.
Sources & evidence
- ORD record
- ord-21e64a67c39e47b2b9d5b84366d65de3
- Source dataset
- uspto-grants-2001_05
- Patent number
- US06231714B1
Reaction notes
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